Reindarstellung von Lanthan- und Praseodym-Ammoniumdoppelnitraten durch fraktionierte Kristallisation in großem Maßstab |
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Authors: | K Rossmanith |
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Institution: | (1) Institut für Anorganische Chemie, Universität Wien, A-1090 Wien, Österreich |
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Abstract: | Summary Lanthanum ammonium nitrate of purity 97%, containing 34.1 kgRE
2O3, was crystallized fractionally and yielded 32.5 kg oxide of purity better than 99.9% (the larger part was 99.99% pure). Out of mixtures with 66% Pr there resulted praseodymium ammonium nitrate containing 13.45 kg oxide of purity better than 99.5%. The effective separation factors are discussed, showing a better efficiency of the ammonium than of the magnesium double nitrates for the separation of praseodymium and lanthanum. |
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Keywords: | Lanthanum ammonium nitrate Praseodymium ammonium nitrate Fractional crystallisation |
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