| XRD谱研究扩散控制的固-固相反应 |
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| 引用本文： | 周益明,叶向荣,李道华,忻新泉.XRD谱研究扩散控制的固-固相反应[J].高等学校化学学报,1999,20(3):361-363. |
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| 作者姓名： | 周益明 叶向荣 李道华 忻新泉 |
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| 作者单位： | 南京大学配位化学研究所,配位化学国家重点实验室,南京,210093 |
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| 摘 要： | 很多分子固体和低维固体在室温或低热温度条件下可发生固相反应［１，２］，甚至可以在短时间内完成［３，４］．我们已成功地用低热固相合成法合成了２００多个化合物，其中大多数为结构新颖的原子簇化合物［５～７］．同时，在每个阶段实验事实的基础上，指出固－固相反...
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| 关 键 词： | 固-固相反应 扩散控制 XRD谱 Schiff碱 |
| 修稿时间： | 1998-03-17． |
Studies on the Diffusion-controlled Solid-solid State Reaction by Means of XRD |
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| ZHOU Yi-Ming,YE Xiang-Rong,LI Dao-Hua,XIN Xin-Quan.Studies on the Diffusion-controlled Solid-solid State Reaction by Means of XRD[J].Chemical Research In Chinese Universities,1999,20(3):361-363. |
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| Authors: | ZHOU Yi-Ming YE Xiang-Rong LI Dao-Hua XIN Xin-Quan |
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| Abstract: | Solid\|solid state condensation reaction of \%p\%\|hydroxybezaldehyde and \%p\%\|chloroaniline was conducted at low\|heating temperature. The reaction product was proved to be the corresponding Schiff base. TG\|DTA and XRD measurements were performed to investigate the solid\|solid state reaction process. It is fairly definite that the reaction is diffusion\|controlled.\= |
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| Keywords: | Solid\|solid state condensation reaction Diffusion\|controlled XRD patterns Schiff base |
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