| 1,3,3a,5-四苯基-3a,4,5,11-四氢-3H,6H-1,2,4-三唑并[4,3-d][1,5]苯并二氮杂(艹卓)的合成及晶体结构 |
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| 引用本文： | 许家喜,金声,张泽莹,麦松威.1,3,3a,5-四苯基-3a,4,5,11-四氢-3H,6H-1,2,4-三唑并[4,3-d][1,5]苯并二氮杂(艹卓)的合成及晶体结构[J].高等学校化学学报,1998,19(7). |
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| 作者姓名： | 许家喜 金声 张泽莹 麦松威 |
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| 摘 要： | 通过2,4-二苯基-2,3-二氢-1H-1,5-苯并二氮杂(艹卓)与苯甲酰氯苯腙的2+3]环加成反应制备了标题化合物,用X射线单晶衍射仪测定了其晶体结构.晶体属正交晶系,空间群为Fdd2.晶胞参数:a=1.762 8(4)nm,b=5.751 2(12)nm,c=1.022 7 nm,V=10.368(5)nm3,Z=16,Dc=1.262 g·cm-3,μ=0.075 mm-1,F(000)=4 160,1 139个可观测衍射点,R-0.046 1,Rw=0.056 0.
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| 关 键 词： | 3a 4 5 11-四氢-3H 6H-1 2 4-三唑并[4 3-d][1 5]苯并二氮杂(艹卓) 晶体结构 分子结构 |
Synthesis and Crystal Structure of 1,3,3a,5-Tetraphenyl-3a,4,5,11-tetrahydro-3H,6H-1,2,4-triazolo [4,3-d][1,5] benzodiazepine |
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| XU Jia-Xi,JIN Sheng,ZHANG Ze-Ying,MAK Thomas C.W..Synthesis and Crystal Structure of 1,3,3a,5-Tetraphenyl-3a,4,5,11-tetrahydro-3H,6H-1,2,4-triazolo [4,3-d][1,5] benzodiazepine[J].Chemical Research In Chinese Universities,1998,19(7). |
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| Authors: | XU Jia-Xi JIN Sheng ZHANG Ze-Ying MAK Thomas CW |
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