| 微波场下水滑石的快速合成及制备 |
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| 引用本文： | 贺鹤鸣,蒋大振.微波场下水滑石的快速合成及制备[J].高等学校化学学报,1992,13(11):1462-1463. |
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| 作者姓名： | 贺鹤鸣 蒋大振 |
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| 作者单位： | 吉林大学化学系 长春130023
(贺鹤鸣，蒋大振)，吉林大学化学系 长春130023(孙铁) |
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| 摘 要： | 水滑石以其独特的碱催化性能~1,2]、记忆效应及阴离子交换~3]等特性引起人们的关注,其合成多用水热法.本文研究了在微波场中水滑石的合成及制备,得到了较好的结果. 1 实验部分 1.1 仪器与试剂 Shimadzu CD-3A型X射线衍射仪(日本);Nicolet 5DX FTIR光谱仪(美国),KBr压片;蚬华E100-EA型微波炉(广东顺德).所有试剂均为分析纯.
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| 关 键 词： | 水滑石 类水滑石 微波 交联 |
Preparation and Synthesis of Hydrotalc in Microwave Field |
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| HE He-Ming,JIANG Da-Zhen,SUN Tie.Preparation and Synthesis of Hydrotalc in Microwave Field[J].Chemical Research In Chinese Universities,1992,13(11):1462-1463. |
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| Authors: | HE He-Ming JIANG Da-Zhen SUN Tie |
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| Abstract: | The present study reports the synthesis of hydrotalc and hydrotalc-like substance by microwave method,which was compared with that of the conventional hydrothermal method.The microwave method gave a good quality product rapidly.By the characterization of XRD and IR,it was found that the hydrotalc can be intercalated easily and exchanged completely with anions.The intercalating products possess a long-range order. |
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| Keywords: | Hydrotalc Hydrotalc-like Microwave Intercalation |
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