| Fe、Si-ZSM-5沸石生成的研究 |
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| 引用本文： | 马淑杰,裘式伦,冯典英,辛敏谦.Fe、Si-ZSM-5沸石生成的研究[J].高等学校化学学报,1987,8(5):393. |
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| 作者姓名： | 马淑杰 裘式伦 冯典英 辛敏谦 |
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| 作者单位： | 吉林大学化学系 |
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| 摘 要： | 本文研究了原始凝胶组成为5Na2O·Fe2O2·(20-150)SiO2·(800-6000)H2O·(30-100) 1,6-己二胺体系晶化过程中固相、液相Fe3+的存在状态,硅酸根离子聚合状态,1,6-己二胺失重情况,固相粒度变化及液相SiO2变化情况。
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| 收稿时间： | 1985-11-16 |
The Study of the Formation of Zeolite Fe-Si-ZSM-5 |
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| Ma Shujie,Qiu Shilun,Feng Dianying,Xin Minqian.The Study of the Formation of Zeolite Fe-Si-ZSM-5[J].Chemical Research In Chinese Universities,1987,8(5):393. |
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| Authors: | Ma Shujie Qiu Shilun Feng Dianying Xin Minqian |
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| Institution: | Department of Chemistry, Jilin University, Changchun |
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| Abstract: | In the course of the crystallization of Fe, Si-ZSM-5 type zeolite with the initial gel composition of 5Na2O·Fe2O2·(20-150)SiO2(800-6000)H2O·(30-100)1,6-HDA we studied the states of existence of Fe3+ions and of polymerization of silicate anions in the solid and the liquid, loss of weight of 1,6-hexadiamine, changes in particle size of solid phase and SiO2in the liquid using ESR,TMS-GC, TG-DTA,electronic microscopy and chemical analysis. |
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