Synthesis and structure of (thio)semicarbazonocyclohexanedicarboxylates. Crystalline and molecular structure of diethyl 4-hydroxy-4-methyl-2-phenyl-6-thiosemicarbazonocyclohexane-1,3-dicarboxylate |
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| Authors: | N V Poplevina A P Kriven’ko O A Shchelochkova A G Golikov S F Solodovnikov |
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| Institution: | 1.Chernyshevskii Saratov State University,Saratov,Russia;2.Saratov State Medical University,Saratov,Russia;3.Nikolaev Institute of Inorganic Chemistry, Siberian Division,Russian Academy of Sciences,Novosibirsk,Russia |
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| Abstract: | Diethyl 2-aryl-4-hydroxy-4-methyl-6-(thio)semicarbazonocyclohexane-1,3-dicarboxylates were synthesized, and their structure
was determined by 1H and 13C NMR spectroscopy, including the HSQC technique. The molecular and crystalline structure of diethyl 4-hydroxy-4-methyl-6-thiosemicarbazono-2-phenylcyclohexane-1,3-dicarboxylate
was determined by X-ray analysis. |
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