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Complete NMR data assignments for novel pterocarpans from Harpalyce brasiliana
Authors:Araújo Renata Mendonça  Pinheiro Sávio Moita  Lima Mary Anne Sousa  Silveira Edilberto Rocha
Institution:Curso de Pós‐Gradua??o em Química Organica, Departamento de Química Organica e Inorganica, Universidade Federal do Ceará, Cx. Postal12200, 60.021‐940, Fortaleza‐CE, Brazil
Abstract:A NMR study of two new pterocarpans isolated from the roots of Harpalyce brasiliana is described. In addition to 1D NMR, 2D shift-correlated NMR pulse sequences ((1)H-(1)H-COSY, HSQC and HMBC) were used to establish the structures, and unambiguously perform the (1)H and (13)C chemical shift assignments.
Keywords:NMR  1H NMR  13C NMR  1D NMR  2D NMR  chemical shift assignments  Harpalyce brasiliana  pterocarpans
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