Total synthesis of gibbilimbols A-D |
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| Authors: | Vyvyan James R Holst Christian L Johnson Allison J Schwenk Cheryl M |
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| Institution: | Department of Chemistry, Western Washington University, Bellingham, Washington 98225-9150, USA. vyvyan@chem.wwu.edu |
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| Abstract: | Gibbilimbols A-D (1-4) were synthesized in 32-49% yield over four steps from commercially available starting materials. A copper-catalyzed coupling of 4-methoxyphenylmagnesium bromide with various unsaturated alkyl bromides was the key step in assembling the (long-chain alkyl)phenol skeleton. |
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