Reactions of aroylpyruvic acids withS-methylisothiosemicarbazide hydroiodide and studies of the crystal structures of the reaction products |
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| Authors: | Z G Aliev L O Atovmyan Yu S Andreichikov S V Kol'tsova D D Nekrasov |
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| Institution: | (1) Institute of Chemical Physics in Chernogolovka, Russian Academy of Sciences, 142432 Chernogolovka, Moscow Region, Russian Federation;(2) Institute of Technical Chemistry, Ural Branch of the Russian Academy of Sciences, 13a ul. Lenina, 614600 Perm, Russian Federation |
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| Abstract: | The reactions ofp-chlorobenzoyl- and benzoylpyruvic acids withS-methylisothiosemicarbazide hydroiodide gave 3-methylthio-6-(p-chlorophenacyl)-2,5-dihydro-1,2,4-triazin-5-one and 6-phenacyl-2,3,4,5-tetrahydro-1,2,4-triazine-3,5,-dione, respectively.
The molecular and crystal structures of the compounds synthesized were studied by X-ray diffraction analysis.
Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 4, pp. 704–708, April, 1998. |
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| Keywords: | aroylpyruvic acids S-methylisothiosemicarbazide hydroiodide 3-methylthio-6-(p-chlorophenacyl)-2 5-dihydro-1 2 4-triazin-5-one 6-phenacyl-2 3 4 5-tetrahydro-1 2 4-triazine-3 5-dione molecular and crystal structure |
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