Solid-state mechanochemical synthesis of tris(4-imino-2-pentanonato)chromium,Cr[CH3C(NH)CHC(O)CH3]3 |
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Authors: | A P Borisov L A Petrova T P Karpova V D Makhaev |
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Institution: | (1) Institute of New Chemical Problems, Russian Academy of Sciences, 142432 Chernogolovka, Moscow Region, Russian Federation |
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Abstract: | Tris(4-imino-2-pentanonato)chromium was prepared by solid-state synthesis under conditions of mechanical activation of a mixture of chromium(III) chloride and sodium 4-imino-2-pentanonate and characterized by IR spectroscopy, X-ray diffraction, and electronic absorption spectroscopy.Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 12, pp. 2227–2229, December, 1994.The present work was carried out as a part of Project No. 1.164 Mechanochemical Synthesis of Complex Compounds of The State Scientific and Technical Program Ecologically Safe Processes in Chemistry and Chemical Technology with the financial support of the Ministry of Science of the RF. |
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Keywords: | chromium complexes acetylacetoneimine mechanochemical synthesis |
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