Synthesis and X-ray study of a bis-diphenylboron chelate of 3-(diaminomethylene)pentane-2,4-dione |
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| Authors: | V A Dorokhoy L G Vorontsova M G Kurella L I Parfenova |
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| Institution: | (1) N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosy., 117913 Moscow, Russian Federation |
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| Abstract: | A bis-diphenylboron chelate has been synthesized from 3-(diaminomethylene)pentane-2,4-dione through the action of (butylthio)diphenylborane and its molecular and crystal structures have been determined. The two boron -containing rings have the same six-membered skeleton but differ substantially in conformation and geometric parameters.Translated fromlzvestiva Akademii Nauk. Seriya Khimicheskaya, No. 11, pp. 2733–2735, November, 1996, |
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| Keywords: | 3-(diaminomethylene)perltane-2 4-dione (butylthio)diphenylboralle diphenylboron chelates X-ray analysis |
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