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Fabrication and physicochemical characterization of graphene oxide derived from thermally expanded graphite
Authors:Email author" target="_blank">L?V?IlkevichEmail author  T?B?Tkachenko  A?V?Samarov  A?A?Burtsev  S?A?Sozinov  L?M?Hitsova  A?N?Popova  Ch?N?Barnakov  A?P?Kozlov
Institution:1.Federal Research Center for Coal and Coal Chemistry,Siberian Branch of the Russian Academy of Sciences,Kemerovo,Russian Federation;2.Kemerovo State University,Kemerovo,Russian Federation;3.Department of Chemistry,M. V. Lomonosov Moscow State University,Moscow,Russian Federation
Abstract:Graphene oxide was obtained from expanded graphite according to the modified Hummers method. The reaction time was significantly reduced (from 24 to 8 h) by applying the expanded graphite in the oxidation process. The interlayer distance in obtained samples was equal to 0.70–0.74 nm. Structural features of the material were studied by the powder X-ray diffraction, thermogravimetric analysis, scanning electron microscopy, transmission electron microscopy, XPS spectroscopy, and NMR spectroscopy.
Keywords:
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