| Stereoselective Synthesis and Crystal Structure Analysis of N-Naphthyl-2-deoxy-α-D-ribopyranosylamine |
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| 引用本文： | 尚培华,成昌梅,杨永冲,王如骥,赵玉芬.Stereoselective Synthesis and Crystal Structure Analysis of N-Naphthyl-2-deoxy-α-D-ribopyranosylamine[J].结构化学,2009(6):761-765. |
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| 作者姓名： | 尚培华 成昌梅 杨永冲 王如骥 赵玉芬 |
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| 作者单位： | Laboratory;Bioorganic;Phosphorus;Chemistry;Chemical;Biology;（Ministry;Education）;Department;Tsinghua;University; |
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| 基金项目： | supported by the National Natural Science Foundation of China (No. 20132020) |
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| 摘 要： | A new compound N-naphthyl-2-deoxy-α-D-ribopyranosylamine was synthesized and structurally determined. It crystallizes in the orthorhombic system, space group P212121 with a = 8.361（2）, b = 12.432（3）, c = 12.791（4） A^°, Z= 4, V= 1329.6（6） A^°^3, Dc= 1.295 g/cm^3, F（000） = 552, Cl5H17NO3 and Mr= 259.30. All the active hydrogen atoms are involved in the formation of hydrogen bonds in the molecule.
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| 关 键 词： | 立体选择性合成 晶体结构分析 萘基 脱氧 新化合物 结构测定 正交晶系 空间群 |
Stereoselective Synthesis and Crystal Structure Analysis of N-Naphthyl-2-deoxy-α-D-ribopyranosylamine |
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| SHANG Pei-Hua CHENG Chang-Mei YANG Yong-Chong WANG Ru-Ji ZHAO Yu-Fen.Stereoselective Synthesis and Crystal Structure Analysis of N-Naphthyl-2-deoxy-α-D-ribopyranosylamine[J].Chinese Journal of Structural Chemistry,2009(6):761-765. |
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| Authors: | SHANG Pei-Hua CHENG Chang-Mei YANG Yong-Chong WANG Ru-Ji ZHAO Yu-Fen |
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| Institution: | Key Laboratory of Bioorganic Phosphorus Chemistry & Chemical Biology (Ministry of Education),Department of Chemistry, Tsinghua University, Beijing 100084, China |
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| Abstract: | A new compound N-naphthyl-2-deoxy-α-D-ribopyranosylamine was synthesized and structurally determined. It crystallizes in the orthorhombic system, space group P212121 with a = 8.361(2), b = 12.432(3), c = 12.791(4) , Z = 4, V = 1329.6(6) 3, Dc = 1.295 g/cm3, F(000) = 552, C15H17NO3 and Mr = 259.30. All the active hydrogen atoms are involved in the formation of hydrogen bonds in the molecule. |
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| Keywords: | N-naphthyl-2-deoxy-α-D-ribopyranosylamine synthesis X-ray diffraction crystal structure |
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