| Crystal Structure and Spectral Characters of 2-（4-Methylbenzoly）-3-（4-chlrolphenyl） -4-（1,2,4-triazole）-5-anilino-thiopene |
| |
| 引用本文： | 许良忠,建方方,曹克广,王忠卫.Crystal Structure and Spectral Characters of 2-（4-Methylbenzoly）-3-（4-chlrolphenyl） -4-（1,2,4-triazole）-5-anilino-thiopene[J].结构化学,2004,23(7):739-742. |
| |
| 作者姓名： | 许良忠 建方方 曹克广 王忠卫 |
| |
| 作者单位： | XU Liang-Zhonga JIAN Fang-Fanga② CAO Ke-Guangb，c WANG Zhong-Weib a (New Materials & Function Coordination Chemistry Laboratory，Qingdao University of Science and Technology，Qingdao 266042，China) b (School of Chemical Industry and Material，Beijing Institute of Technology，Beijing 100081，China) c (Chengde Petroleum College，Chengde 067000，China) |
| |
| 基金项目： | This work was supported by the Natural Science Foundation of Shandong Province (No. Y2002B06) |
| |
| 摘 要： | 1 INTRODUCTION The triazole derivatives were widely studied because they represent the largest group of modern fungicides and extensively used in both human and veterinary therapy and in agriculture1～3]. For exam- ple, there are commercially available …
|
| 关 键 词： | 晶体结构 光谱特征 硫代喷丸 1 2 4-三唑 甲苯基 氢键 |
Crystal Structure and Spectral Characters of 2-(4-Methylbenzoly)-3-(4-chlrolphenyl)-4-(1,2,4-triazole)-5-anilino-thiopene |
| |
| Abstract: | The title compound 2-(4-methylbenzoly)-3-(4-chlrolphenyl)-4-(1,2,4-triazole)-5-anilino-thiopene has been prepared and characterized by IR,EA,1H NMR,UV,MS and X-ray analysis.It crystallizes in the triclinic system,space group P with a = 8.061(2),b = 9.981(2),c = 15.462(3)(A) ,α = 90.96(3),β = 103.11(3),γ = 106.26(3)o,Mr = 470.96 (C26H19ClN4OS),V = 1158.8(4)(A)3,Z = 2,Dc = 1.350 g/cm3,F(000) = 488,μ = 0.282 mm-1,R = 0.0482 and Wr = 0.1043.In the crystal lattice,there exist some intermolecular hydrogen bonds,π-π stacking interactions and C-H··π supramolecular interactions.In the solid state,all of the above intermolecular interactions in the title compound can stabilize the crystal structure. |
| |
| Keywords: | crystal structure thiopene 1 2 4-triazole hydrogen bond |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
