Synthesis, Crystal Structure and Fluorescent Property of a New Sulfanilamide Schiff-base Compound |
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| Authors: | TANG Yun-Zhi WEN He-Rui ZHANG Jian TAN Yu-Hui |
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| Institution: | 1. School of Material Science & Chemistry Engineering,Jiangxi University of Science and Technology,Ganzhou 341000,China
2. Department of Pharmacy,Gannan Medical University,Ganzhou 341000,China |
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| Abstract: | A new sulfanilamide Schiff-base compound N,N'-(p-phenyl sulfanilamide)-5,6-dimethoxy-pyrimidine-(2-hydroxyl benzene)methylidene has been synthesized by the condensation of equimolar salicylaldehyde and 4-(p-amino phenyl sulfanilamide)-5,6-dimethoxy-pyrimidine in an anhydrous ethanol solution.The compound was characterized by elemental analysis,IR spectra,and single-crystal X-ray diffraction.The crystal belongs to the monoclinic system,space group P2_1/c witha=19.0425(11),b=11.1914(6),c=9.0075(5)(A),β=93.9650(10)°,Z=4,ν=1915.01(18)(A)~3,D_c=1.437g/cm~3,M_r=414.43,2(MoKa)=0.71073(A),μ=2.09mm~(-1),F(000)=864,R=0.0385 and wR=0.1224. |
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| Keywords: | Schiff base sulfanilamide crystal structure fluorescent property |
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