| CRYSTAL AND MOLECULAR STRUCTURE OF (μ-PhS)-(μ-p-CH_3C_6H_4CCH=CH) Fe_2(CO)6 |
| |
| 基金项目： | Project supported by the National Science Foundation of China |
| |
| 摘 要： | <正> The red transparent crystals of the title complex C22H14O7SFe2 (Mr=534.0996) crystallize in triclinic space group Flwith cell parameters:a = 9. 939(6),b= 10. 065(5), c= 12. 344(7) A;a=73. 95(4),B=79. 07(4),y=74. 77(4) ;V= 1135. 87A;Z=2;Dc=1.56g.cm-3;F(000) = 540. 0. The final R and Rwis 0.089 and 0. 086 for 3051 observed unique reflections. The ligand u-a,n-p-CH3C6H4C(O)CH=CH in the title complex is coordinated to two Fe atoms.
|
CRYSTAL AND MOLECULAR STRUCTURE OF (μ-PhS)-(μ-p-CH_3C_6H_4CCH=CH) Fe_2(CO)6 |
| |
| Abstract: | The red transparent crystals of the title complex C22H14O7SFe2 (Mr=534.0996) crystallize in triclinic space group Flwith cell parameters:a = 9. 939(6),b= 10. 065(5), c= 12. 344(7) A;a=73. 95(4),B=79. 07(4),y=74. 77(4) ;V= 1135. 87A;Z=2;Dc=1.56g.cm-3;F(000) = 540. 0. The final R and Rwis 0.089 and 0. 086 for 3051 observed unique reflections. The ligand u-a,n-p-CH3C6H4C(O)CH=CH in the title complex is coordinated to two Fe atoms. |
| |
| Keywords: | |
| 本文献已被 CNKI 等数据库收录！ |
|
