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Synthesis and Structure of the Hexanuclear Diazenido-oxomolybdate [(n-C_4H_9)_4N]_3[Mo_6O_(18)(N_2C_6H_4-p-NO_2)]
引用本文:Li Hai-Lian,You Xiao-Zeng,Xu Xue-Xiang(Coordination Chemistry Institute,State Key Laboratory ofCoordination Chemistry,Nanjing,210008)Huang Jin-Shun(State Key Laboratory of Structural Chemistry,Fuzhou,350002). Synthesis and Structure of the Hexanuclear Diazenido-oxomolybdate [(n-C_4H_9)_4N]_3[Mo_6O_(18)(N_2C_6H_4-p-NO_2)][J]. 结构化学, 1994, 0(2)
作者姓名:Li Hai-Lian  You Xiao-Zeng  Xu Xue-Xiang(Coordination Chemistry Institute  State Key Laboratory ofCoordination Chemistry  Nanjing  210008)Huang Jin-Shun(State Key Laboratory of Structural Chemistry  Fuzhou  350002)
作者单位:Li Hai-Lian;You Xiao-Zeng;Xu Xue-Xiang(Coordination Chemistry Institute,State Key Laboratory ofCoordination Chemistry,Nanjing,210008)Huang Jin-Shun(State Key Laboratory of Structural Chemistry,Fuzhou,350002)
摘    要:SynthesisandStructureoftheHexanuclearDiazenido-oxomolybdate[(n-C_4H_9)_4N]_3[Mo_6O_(18)(N_2C_6H_4-p-NO_2)]LiHai-Lian;YouXiao-Zeng;...


Synthesis and Structure of the Hexanuclear Diazenido-oxomolybdate[(n-C_4H_9)_4N]_3[Mo_6O_(18)(N_2C_6H_4-p-NO_2)]
Li Hai-Lian,You Xiao-Zeng,Xu Xue-Xiang. Synthesis and Structure of the Hexanuclear Diazenido-oxomolybdate[(n-C_4H_9)_4N]_3[Mo_6O_(18)(N_2C_6H_4-p-NO_2)][J]. Chinese Journal of Structural Chemistry, 1994, 0(2)
Authors:Li Hai-Lian  You Xiao-Zeng  Xu Xue-Xiang
Abstract:Compound[(n-C4H9)4N]3 [Mo6O18(N2C6H4-pNO2)] crystallizes in the orthorhombic space grou Pnma with a= 23. 964(9).b=16.948(4),c=17.968(7) A,V=7298(7) A3,Z=4,and Dc=1.58 g/cm-3. Structure solution and refinement based on 3113 reflections with I>3.0σ(I) gave final residuals of R= 0.072 and Rω=0.099.The anion is a substitution isopolymolybdate.
Keywords:synthesis  crystal structure  hexanuclear Mo complex
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