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Syntheses and Structural Characterization of 1-(4-Phenyl-2-thiazolyl)-3-(4-methylphenyl)-5-(2-furyl)-4,5-dihydro-(1H)-pyrazole and 1-(4-(4-Fluoro)phenyl-2-thiazolyl)-3-(4-methyl-phenyl)-5-(2-furyl)-4,5-dihydro-(1H)-pyrazole
作者姓名:AHIN Zarife Sibel  ISIK Samil  SALGIN-GOKSEN Umut  GOKHAN-KELEKCI Nesrin
作者单位:(S)AH(I)N Zarife Sibel,I(S)IK (S)amil(Department of Physics,Faculty of Arts and Sciences,Ondokuz Mayts University,Kurupelit,55139 Samsun,Turkey);SALGIN-G(O)K(S)EN Umut,G(O)KHAN-KELEK(C)(I) Nesrin(Department of Pharmaceutical Chemistry,Faculty of Pharmacy,Hacettepe University,06100 Ankara,Turkey) 
基金项目:The authors acknowledge the Faculty of Arts and Sciences, Ondokuz Mayis University, Turkey, for the use of the Stoe IPDSII diffractometer (purchased under grant No. F279 of the University Research Fund)
摘    要:The title compounds were synthesized and characterized by IR,1H-NMR,Mass and elementary analysis and single-crystal X-ray diffraction.In 1a,intermolecular C-H…π interactions produce a three-dimensional network.In 1b,intermolecular C-H…O hydrogen bonds generate an R22(22) ring.The hydrogen bonding is supported by C-H…π interactions.

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Syntheses and Structural Characterization of 1-(4-Phenyl-2-thiazolyl)-3-(4-methylphenyl)-5-(2-furyl)-4,5-dihydro-(1H)-pyrazole and 1-(4-(4-Fluoro)phenyl-2-thiazolyl)-3-(4-methylphenyl)-5-(2-furyl)-4,5-dihydro-(1H)-pyrazole
AHIN Zarife Sibel,ISIK Samil,SALGIN-GOKSEN Umut,GOKHAN-KELEKCI Nesrin.Syntheses and Structural Characterization of 1-(4-Phenyl-2-thiazolyl)-3-(4-methylphenyl)-5-(2-furyl)-4,5-dihydro-(1H)-pyrazole and 1-(4-(4-Fluoro)phenyl-2-thiazolyl)-3-(4-methylphenyl)-5-(2-furyl)-4,5-dihydro-(1H)-pyrazole[J].Chinese Journal of Structural Chemistry,2010,29(5):700-705.
Authors:AHN Zarife Sibel  IIK amil  SALGIN-GKEN Umut  GKHAN-KELEK Nesrin
Institution:1. Department of Physics,Faculty of Arts and Sciences,Ondokuz Mayts University,Kurupelit,55139 Samsun,Turkey
2. Department of Pharmaceutical Chemistry,Faculty of Pharmacy,Hacettepe University,06100 Ankara,Turkey
Abstract:The title compounds were synthesized and characterized by IR, 1H-NMR, Mass and elementary analysis and single-crystal X-ray diffraction. In 1a, intermolecular C-H…π interactions produce a three-dimensional network. In 1b, intermolecular C-H…O hydrogen bonds generate an R22(22) ring. The hydrogen bonding is supported by C-H…π interactions.
Keywords:crystal structure  methylphenyl  pyrazole
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