| Synthesis and Molecular Structure of 1-Acetyl-1-（4-iodophenyl）-3-cyclohexylurea |
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| 引用本文： | 钱秋峰,邹建平,穆学军,曾润生.Synthesis and Molecular Structure of 1-Acetyl-1-（4-iodophenyl）-3-cyclohexylurea[J].结构化学,2006,25(1):100-102. |
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| 作者姓名： | 钱秋峰 邹建平 穆学军 曾润生 |
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| 作者单位： | Key Laboratory of Organic Synthesis of Jiangsu Province College of Chemistry and Chemical Engineering Suzhou University Suzhou 215006 Jiangsu China，Key Laboratory of Organic Synthesis of Jiangsu Province College of Chemistry and Chemical Engineering Suzhou University Suzhou 215006 Jiangsu China，Key Laboratory of Organic Synthesis of Jiangsu Province College of Chemistry and Chemical Engineering Suzhou University Suzhou 215006 Jiangsu China，Key Laboratory of Organic Synthesis of Jiangsu Province College of Chemistry and Chemical Engineering Suzhou University Suzhou 215006 Jiangsu China |
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| 摘 要： | 1INTRODUCTION N-acyl urea is an important class of compounds because of their various bioactivities,and they can be used as pesticides1]and pharmaceuticals2].On the other hand,many natural products bearing N-acylurea functionality also exhibit the inter…
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| 关 键 词： | 合成 分子结构 1-乙酰基碘苯基-3-环己基尿素 X射线衍射研究 |
Synthesis and Molecular Structure of 1-Acetyl-1-(4-iodophenyl)-3-cyclohexylurea |
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| QIAN Qiu-Feng,ZOU Jian-Ping,MU Xue-Jun,ZENG Run-Sheng.Synthesis and Molecular Structure of 1-Acetyl-1-(4-iodophenyl)-3-cyclohexylurea[J].Chinese Journal of Structural Chemistry,2006,25(1):100-102. |
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| Authors: | QIAN Qiu-Feng ZOU Jian-Ping MU Xue-Jun ZENG Run-Sheng |
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| Institution: | Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215006, Jiangsu, China |
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| Abstract: | The title compound 1-acetyl-1-(4-iodophenyl)-3-cyclohexylurea 1 (C15H19IN2O2, Mr = 386.22) has been synthesized and its crystal structure was determined by X-ray diffraction analysis. It crystallizes in orthorhombic, space group Pbca, a =15.4754(16), b = 11.4284(11), c = 17.829(2) (A),Z = 8, V = 3153.2(6)(A)3, Dc= 1.627 mg/m3, μ(MoKα) = 2.034 mm-1, F(000) = 1536, the final R = 0.0276 and wR = 0.0593 for 2805 observed reflections (I > 2σ(I)). X-ray analysis reveals that cyclohexyl ring adopts a chair conformation, with the cyclohexyl group located at the 3-position of urea, and the acetyl and 4-iodophenyl groups at the 1-position. |
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| Keywords: | 1-acetyl-1-(4-iodophenyl)-3-cyclohexylurea synthesis crystal structure |
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