| Crystal Structure of trans－2－（1－Naphthyl）－1－（p－（4＇，4＇，5＇，5＇－tetramethyl－4＇，5＇－dihydro－1＇H－imidazolyl－1＇－oxy－3＇－oxide）－phenyl）－imine，C_（24）H_（24）N_3O_2 |
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| 作者姓名： | Zhang Bin Zhang De-Qing Zhu Dao-Ben |
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| 作者单位： | Institute of Chemistry，Academia Sinica，Beijing 100080 |
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| 摘 要： | ＣｒｙｓｔａｌＳｔｒｕｃｔｕｒｅｏｆｔｒａｎｓ－２－（１－Ｎａｐｈｔｈｙｌ）－１－（ｐ－（４＇，４＇，５＇，５＇－ｔｅｔｒａｍｅｔｈｙｌ－４＇，５＇－ｄｉｈｙｄｒｏ－１＇Ｈ－ｉｍｉｄａｚｏｌｙｌ－１＇－ｏｘｙ－３＇－ｏｘｉｄｅ）－ｐｈｅｎｙｌ）－ｉｍ...
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Crystal Structure of trans-2-(1-Naphthyl)-1-(p-(4',4',5',5'-tetramethyl-4',5'-dihydro-1'H-imidazolyl-1'-oxy-3'-oxide)-phenyl)- imine,C_(24)H_(24)N_3O_2 |
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| Zhang Bin,Zhang De-Qing,Zhu Dao-Ben.Crystal Structure of trans-2-(1-Naphthyl)-1-(p-(4'''',4'''',5'''',5''''-tetramethyl-4'''',5''''-dihydro-1''''H-imidazolyl-1''''-oxy-3''''-oxide)-phenyl)- imine,C_(24)H_(24)N_3O_2[J].Chinese Journal of Structural Chemistry,1994(5). |
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| Authors: | Zhang Bin Zhang De-Qing Zhu Dao-Ben |
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| Abstract: | The crystal structure of the title compound was determined by X-ray diffraction method at room temperature.The crystal belongs to triclinic space group P1 with the following crystallographic parameters:a=13.942(2),b=15.540(2),c=10.007(1) A,a=105.16(1)°,β=92.42(1)°,γ=88.12(1)°,V=2090.2(4) Z=4,Dc=1.23g cm-3,F(000)=820,μ(MoKα)=0.74 cm-1,and final R= 0.054 for 3208 observations.Two molecules , which are slightly different in conformation,coexist in an asymmetric unit. Some intermolecular distances are fairly short.The packing arrangement of the molecules in the crystal is also discussed. |
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| Keywords: | crystal structure nitroxyl free radical organic compound organic ferromagnetism |
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