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A normal phase HPTLC method for the quantitative determination of ochratoxin A in rice
Authors:M Dawlatana  R D Coker  M J Nagler  G Blunden
Institution:(1) Institute of Food Science and Technology, Bangladesh Council of Scientific and Industrial Research, New Elephant Road, 1205 Dhaka, Bangladesh;(2) Natural Resources Institute, Chatham Maritime, Central Avenue, ME4 4TB Chatham, Kent, UK;(3) School of Pharmacy and Biomedical Sciences, University of Portsmouth, King Henry I Street, PO1 2DZ Portsmouth, UK
Abstract:Summary A previously published 1] liquid chromatographic method for the determination of ochratoxin A in corn, barley and kidney has been modified for application to parboiled rice with quantification by high performance thin layer chromatography (HPTLC). The method has been validated by spiking uncontaminated extracts of rice with ochratoxin A over the range 0 to 198 mgrg kg–1. The proposed method has some significant advantages over the current AOAC method 2], especially for determining low levels of ochratoxin A in parboiled rice.
Keywords:High-performance thin-layer chromatography (HPTLC)  Solid phase extraction  Parboiled rice  Ochratoxin A
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