| 微乳液和均匀沉淀耦合法制备CeO2纳米粒子 |
| |
| 引用本文： | 贺拥军,杨伯伦.微乳液和均匀沉淀耦合法制备CeO2纳米粒子[J].化学通报,2003,66(2):120-124. |
| |
| 作者姓名： | 贺拥军 杨伯伦 |
| |
| 作者单位： | 贺拥军（西安交通大学环境与化工学院,西安,710049）;杨伯伦（西安交通大学环境与化工学院,西安,710049） |
| |
| 基金项目： | 陕西省自然科学基金资助项目 |
| |
| 摘 要： | 用W/O微乳液和草酸二甲酯均匀沉淀耦合法制备出单分散性好并具有较窄粒度分布的CeO2纳米粒子,测试了其形貌、粒径及粒径分布和晶体结构等特征.实验结果表明,表面活性剂的种类和反应物的相对初始浓度对产物平均粒径具有规律性的影响;随着焙烧温度升高,产物的平均粒径明显增大.
|
| 关 键 词： | 微乳液 均匀沉淀 纳米 二氧化铈 |
| 修稿时间： | 2002年6月6日 |
The Synthesis of Nanometer Sized CeO2 Particles by the Coupling Route of Microemulsion with Homogeneous Precipitation |
| |
| He Yongjun,Yang Bolun.The Synthesis of Nanometer Sized CeO2 Particles by the Coupling Route of Microemulsion with Homogeneous Precipitation[J].Chemistry,2003,66(2):120-124. |
| |
| Authors: | He Yongjun Yang Bolun |
| |
| Institution: | He Yongjun,Yang Bolun * |
| |
| Abstract: | CeO 2 nanoparticles with good monodispersity and narrow size distribution were synthesized by the coupling route of W/O microemulsion with homogenous precipitation. The morphology, size, size distrbution and the crystal structure of CeO 2 nanoparticles were inspected. It was found that the sort of surfactants and the relative initial concentration of reactants have regular affections on the average size of products. The average size of products increases sharply with the calcination temperature. Research results may present a promising method for the synthesis of nanoparticles with controlled size and size distribution. |
| |
| Keywords: | Microemulsion Homogenous precipitation Nanometer Cerium dioxide |
| 本文献已被 CNKI 等数据库收录！ |
|
