| 1-[4-(1,2,4-三唑-5-硫酮)]-3-对甲氧基苯甲酰基硫脲镍配合物的晶体结构 |
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| 引用本文： | 张鹏娟,黄洁,宋纪蓉,宋媛,徐海霞.1-[4-(1,2,4-三唑-5-硫酮)]-3-对甲氧基苯甲酰基硫脲镍配合物的晶体结构[J].化学通报,2009,72(9). |
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| 作者姓名： | 张鹏娟 黄洁 宋纪蓉 宋媛 徐海霞 |
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| 作者单位： | 张鹏娟,黄洁,宋媛,徐海霞(西北大学化工学院/陕西省物理无机化学重点实验室,西安,710069);宋纪蓉(西北大学化工学院/陕西省物理无机化学重点实验室,西安,710069;故宫博物院文保科技部,北京,100009) |
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| 基金项目： | 国家自然科学基金项目，陕西省自然科学基金项目 |
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| 摘 要： | 采用缓慢蒸发法培养出化合物1-4-(1,2,4-三唑-5-硫酮)]-3-对甲氧基苯甲酰基硫脲镍配合物晶体,并通过X-射线单晶衍射法测定了晶体结构,它为P2/n空间群的单斜晶体,晶胞参数为α=1.2577(2)nm,b=0.88790(17)nm,c=1.2628(2)nm,V=1.3304(4)nm3,R1=0.0291和wR2=0.0694.
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| 关 键 词： | 4-三唑-5-硫酮)]-3-对甲氧基苯甲酰苯硫脲镍 配合物 晶体结构 |
Synthesis and Crystal Structure of Ni(C_(11)H_(12)N_5O_2S_2)_2 Complex |
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| Zhang Pengjuan,Huang Jie ,Song Jirong ,Song Yuan,Xu Haixia.Synthesis and Crystal Structure of Ni(C_(11)H_(12)N_5O_2S_2)_2 Complex[J].Chemistry,2009,72(9). |
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| Authors: | Zhang Pengjuan Huang Jie Song Jirong Song Yuan Xu Haixia |
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| Institution: | ~1 College of Chemical Engineering/Shaanxi Key Laboratory of Physico-Inorganic Chemistry;Northwest University;Xi'an 710069;~2 Conservation Technology Department;the Palace Museum;Beijing 100009 |
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| Abstract: | The single crystals of the complex Ni (C_ 11 H_ 12 N_5O_2S_2)_2 was obtained by slow evaporation method at room temperature and its crystal structure was determined with a X-ray diffractometer. It is a monoclinic crystal,its crystallographic parameters are P2/n space group with a=1.2577(2)nm,b= 0.88790(17)nm,c=1.2628(2)nm,V=1.3304(4)nm~3,R_1=0.0291 and wR_2=0.0694. |
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| Keywords: | 1-[4-(1 2 |
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