| NaBF4催化合成二吲哚甲烷类化合物 |
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| 引用本文： | 谢宗波,孙大召,陈中胜,乐长高.NaBF4催化合成二吲哚甲烷类化合物[J].化学通报,2015,78(8):757-760. |
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| 作者姓名： | 谢宗波 孙大召 陈中胜 乐长高 |
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| 作者单位： | 东华理工大学应用化学系,东华理工大学应用化学系,东华理工大学应用化学系,东华理工大学应用化学系 |
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| 摘 要： | 在乙醇水溶液中,以Na BF4为催化剂,通过吲哚与芳香醛间的串联反应合成了二吲哚甲烷衍生物。考察了催化剂种类、反应介质、温度、反应时间等因素对反应的影响,在优化条件下以较高产率得到了一系列目标产物。
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| 关 键 词： | NaBF4 乙醇水溶液 二吲哚甲烷 串联反应 |
| 收稿时间： | 2015/2/10 0:00:00 |
| 修稿时间： | 2015/3/17 0:00:00 |
Synthesis of Bis(indolyl)alkanes Catalyzed by Sodium Fluoroborate |
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| xie zong bo,Sun Dazhao,Chen Zhongsheng and Le ZhangGao.Synthesis of Bis(indolyl)alkanes Catalyzed by Sodium Fluoroborate[J].Chemistry,2015,78(8):757-760. |
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| Authors: | xie zong bo Sun Dazhao Chen Zhongsheng and Le ZhangGao |
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| Abstract: | A cascade reaction catalyzed by NaBF4 was firstly reported for the synthesis of bis(indolyl)methanes starting from indole and aromatic aldehydes in ethanol aqueous solution. The reaction conditions was optimized with catalyst, medium, temperature and reaction time, and a series of bis(indolyl)alkanes were obtained in moderate to good yields under the optimal reaction conditions. |
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| Keywords: | NaBF4 ethanol aqueous solution bis(indolyl)alkane cascade reaction |
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