| 二甲基烯丙基胺/溴代烷烃系列季铵盐的合成与表征 |
| |
| 引用本文： | 赵文善,张磊,崔元臣,茹阳.二甲基烯丙基胺/溴代烷烃系列季铵盐的合成与表征[J].化学研究,2011,22(6):49-51. |
| |
| 作者姓名： | 赵文善 张磊 崔元臣 茹阳 |
| |
| 作者单位： | 河南大学化学化工学院,河南开封,475004 |
| |
| 摘 要： | 以溴代烷与二甲基烯丙基胺(DMAA)为原料合成了二甲基烯丙基类季铵盐；探讨了反应温度、原料配比、反应时间及溶剂对反应产率的影响,确定了最佳合成条件；并采用红外光谱仪、核磁共振谱仪(1 H NMR)及质谱仪表征了产物的结构.
|
| 关 键 词： | 二甲基乙基烯丙基溴化铵 二甲基正丁基烯丙基溴化铵 季铵盐 |
Synthesis and characterization of quaternary ammonium salts of dimethylallylamine/bromoalkane |
| |
| ZHAO Wen-shan,ZHANG Lei,CUI Yuan-chen,RU Yang.Synthesis and characterization of quaternary ammonium salts of dimethylallylamine/bromoalkane[J].Chemical Research,2011,22(6):49-51. |
| |
| Authors: | ZHAO Wen-shan ZHANG Lei CUI Yuan-chen RU Yang |
| |
| Institution: | ZHAO Wen-shan,ZHANG Lei,CUI Yuan-chen,RU Yang (College of Chemistry and Chemical Engineering,Henan University,Kaifeng 475004,Henan,China) |
| |
| Abstract: | Dimethylallylamine bromide quaternary ammonium salts were synthesized by using dimethylallylamine and bromoalkane as the starting materials.The effects of reaction temperature,ratio of reactants,reaction time and solvents on the yield of target products were investigated,and the optimum reaction conditions were established.In the meantime,the structure of as-synthesized products was characterized by means of infrared spectrometry,nuclear magnetic resonance spectroscopy(1H NMR) and mass spectrometry. |
| |
| Keywords: | dimethylethylallylammonium bromide dimethylbutylallylammonium bromide quaternary ammonium salts |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
