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芹菜籽香气成分研究
引用本文:陆占国,张怀涛,苏荣军.芹菜籽香气成分研究[J].化学研究,2008,19(2):58-62.
作者姓名:陆占国  张怀涛  苏荣军
作者单位:哈尔滨商业大学,食品工程学院,化学中心,黑龙江,哈尔滨,150076
摘    要:采用固相微萃取法萃取黑龙江产芹菜籽香气成分,然后用GC—MS进行成分分析,并与水蒸气蒸馏法获得的精油成分进行比较.用CAR on PDMS萃取柱进行顶空固相微萃取时,共检测出26种成分,鉴定出占总成份89.650%的20种成分,主要成分为柠檬烯(35.980%),β-月桂烯(20.500%),β-蛇床烯(16.160%),正戊基苯(5.295%),β-蒎烯(3.412%),α-蛇床烯(3.293%).水蒸汽蒸馏法提取芹菜籽,以1.18%产率获得精油,共检测出23个成分,鉴定出占总精油91.375%的18种成分,主要成分为柠檬烯(31.149%),β-蛇床烯(22.281%),对甲苯基异戊酸酯(14.944%),α-2-丙烯基苯甲醇(9.872%),β-月桂烯(4.324%)和α-蛇床烯(4.322%).

关 键 词:芹菜  芹菜籽  固相微萃取  精油  GC-MS

Study on Aromatic Components of Celery Seeds
LU Zhan-guo,ZHANG Huai-tao,SU Rong-jun.Study on Aromatic Components of Celery Seeds[J].Chemical Research,2008,19(2):58-62.
Authors:LU Zhan-guo  ZHANG Huai-tao  SU Rong-jun
Institution:(Chemical Center, School of Food Engineering, Harbin University of Commerce, Harbin 150076, Heilongjiang, China)
Abstract:Aromatic components of the celery seeds grown in Heilongjiang Province were analyzed by using solid phase microextraction combined with GC-MS and compared with the components of the essential oil.When using CAR on PDMS column,a total of 26 components were detected,in which 20 compounds that account for 89.650 % of the total were identified.The main constituents were limonene(35.98 %),β-myrcene(20.500 %),β-selinene(16.160 %),n-pentylbenzene(5.295 %),β-pinene(3.412 %) and α-selinene(3.293 %).The essential oil was obtained by steam distillation extraction method in 1.18 % yield,A total of 23 constituents were detected,in which 18 compounds that account for 91.375 % were identified.The main constituents were limonene(31.149 %),β-selinene(22.281 %),p-cresyl isovalerate(14.944 %), α-2-propenylbenzenemethanol(9.872 %),β-myrcene(4.324 %) and α-selinene(4.322 %).
Keywords:Apium graveolens L  celery seed  solid phase microextraction  essential oil  GC-MS
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