Preparation and Characterization of Polysulfone/Nanosilver-Doped Activated Carbon Nanocomposite |
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Authors: | Jui-Ting Sun Chyung-Chyung Wang Hsun-Tsing Lee Cheng-Lung Wu Jia-Hao Gu Maw-Cherng Suen |
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Institution: | 1.Department of Textile Engineering,Chinese Culture University,Taipei,Taiwan, Republic of China;2.Department of Materials Science and Engineering,Vanung University,Jongli, Taoyuan,Taiwan, Republic of China;3.Department of Materials Science and Engineering,National Taiwan University of Science and Technology,Taipei,Taiwan, Republic of China;4.Department of Fashion Administration and Management,Lee-Ming Institute of Technology,Taishan, New City Taipei,Taiwan, Republic of China |
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Abstract: | In this study, nano silver-doped activated carbon (Ag/C) acted as an inorganic additive and was blended with a polysulfone (PSF) matrix in a tetrahydrofuran (THF) solution, thereby forming nano silver- doped activated carbon/polysulfone (Ag/C/PSF) composites. Subsequently, the silver content and characterization of the Ag/C were identified using energy-dispersive X-ray spectroscopy (EDS), scanning electron microscopy (SEM), and X-ray diffraction (XRD). The FTIR, XRD, EDS and SEM were used to characterize the structure and morphology of the Ag/C/PSF composites. The FTIR spectra analysis revealed that adding a small volume of Ag/C in a PSF matrix did not substantially affect the functional groups of the matrix. The XRD results showed that the characteristic crystallization peaks of Ag/C/PSF (2θ = 26°) increased as the Ag/C content increased. The EDS results revealed that silver elements were inlaid into Ag/C/PSF composites, and the SEM results demonstrated strong interfacial interaction between the Ag/C particles and PSF matrix. The results of thermogravimetric analysis and differential scanning calorimetry appeared that adding Ag/C particles increased the thermal decomposition temperature and glass transition temperature of the Ag/C/PSF composites. From a stress–strain analysis, the added Ag/C particles enhanced the tensile strength of the PSF matrix. The results of contact-angle and atomic-force microscopy measuring showed that the hydrophobicity and surface roughness increased when Ag/C content increased. The antibacterial test results revealed that the Ag/C/PSF composites exhibited excellent antibacterial activity against both Staphylococcus aureus and Escherichia coli. In addition, the electrical conductivity measurements showed that volume resistivity of the Ag/C/PSF composites decreased with the amount of Ag/C increase. |
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