Thermal properties of zinc butyrate complex compounds |
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Authors: | K Györyová V Balek B H Behrens A Matuschek A Kettrup |
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Institution: | (1) Department of Inorganic Chemistry, P. J. Safarik University, Moyzesova 11, 041 54 Kosice, Slovak Republic;(2) Nuclear Research Institute, 250 68 Rez, Czech Republic;(3) Department of Inorganic and Analytical Chemistry, Freie Universität, Fabeck Str. 34-36, 141 95 Berlin;(4) Institut für Ökologische Chemie, 857 58 München-Oberschleissheim, Germany |
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Abstract: | The new zinc(II) complexes of general formula Zn(CH3CH2CH2COO)2· nL (whereL = caffeine, nicotinamide, theobromine;n=1 or 2) were prepared and identified.Thermal properties of these compounds were investigated by thermal analysis (TG/DTG, DTA, DSC/DDSC).Gaseous products of thermal decomposition were detected by IR spectroscopy and Mass spectroscopy. Final products of thermal decomposition were determined by X-ray powder diffraction patterns.This work was supported by the Slovak Ministry of Education Grant No. 1/3230/96. This financial support is gratefully acknowledged. |
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Keywords: | caffeine nicotinamide theobromine thermal properties zinc butyrate |
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