| 二维核磁共振技术解析盐酸帕罗西汀 |
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| 引用本文： | 毛侦军.二维核磁共振技术解析盐酸帕罗西汀[J].分析测试技术与仪器,2022,28(1):31-36. |
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| 作者姓名： | 毛侦军 |
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| 作者单位： | 浙江大学 化学系，浙江 杭州 310058 |
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| 摘 要： | 报道了盐酸帕罗西汀的分子结构解析方法,利用国产核磁共振波谱仪测试了盐酸帕罗西汀核磁氢谱(^(1)H-NMR)、核磁碳谱(^(13)C-NMR、DEPT 135°)、二维核磁相关谱(^(1)H-^(1)HCOSY、^(13)C-^(1)H HSQC、^(13)C-^(1)H HMBC),实现了盐酸帕罗西汀氢碳的全部归属.
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| 关 键 词： | 二维核磁 结构解析 盐酸帕罗西汀 |
| 收稿时间： | 2022-01-25 |
Analysis of Paroxetine Hydrochloride Using 2D-Nuclear Magnetic Resonance |
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| MAO Zhen-jun.Analysis of Paroxetine Hydrochloride Using 2D-Nuclear Magnetic Resonance[J].Analysis and Testing Technology and Instruments,2022,28(1):31-36. |
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| Authors: | MAO Zhen-jun |
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| Institution: | Chemistry Department, Zhejiang University, Hangzhou 310058, China |
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| Abstract: | The molecular structure analysis method of paroxetine hydrochloride was reported. The nuclear magnetic hydrogen spectrum (1H-NMR), nuclear magnetic carbon spectrum (13C-NMR, DEPT 135°) and two-dimensional nuclear magnetic correlation spectrum (1H-1HCOSY, 13C-1H HSQC, 13C-1H HMBC) of paroxetine hydrochloride were measured on the domestic scientific instrument nuclear magnetic resonance spectrometer, and all the hydrogen and carbon of paroxetine hydrochloride were attributed. |
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