气相色谱法测定烟草浸膏中的烟碱 |
| |
引用本文: | 肯生叶,段勤,苏丹丹,杨屹,田飞宇,杨雪燕.气相色谱法测定烟草浸膏中的烟碱[J].分析测试技术与仪器,2022,28(2):205-209. |
| |
作者姓名: | 肯生叶 段勤 苏丹丹 杨屹 田飞宇 杨雪燕 |
| |
作者单位: | 云南养瑞科技集团有限公司, 云南 昆明 650224 |
| |
摘 要: | 为准确测定烟草浸膏中烟碱含量,以2-甲基喹啉为内标建立了测定烟草浸膏中烟碱的气相色谱-氢火焰离子化法(GC-FID),并测定了5个烟草浸膏样品.结果表明,方法的回收率为95.00%~98.58%,检出限为0.27 mg/g,定量限为0.89 mg/g.所测烟草浸膏中烟碱的质量分数在19.66~54.97 mg/g之间.方法简单、灵敏、准确,适用于烟草浸膏中烟碱的测定.
|
关 键 词: | 气相色谱法 烟草浸膏 烟碱 |
收稿时间: | 2022-03-08 |
Determination of Nicotine in Tobacco Concrete by Gas Chromatography |
| |
Institution: | Yunnan Yangrui Technology Group Co. Ltd., Kunming 650224, China |
| |
Abstract: | A gas chromatography-flame ionization (GC-FID) method has been developed for the determination of nicotine in the tobacco concrete using 2-methylquinoline as the internal standards, five tobacco concrete samples were determined. The results showed that the limit of detection and limit of quantitation were 0.27 mg/g and 0.89 mg/g, respectively. The recoveries were 95.00%~98.58%. The contents of nicotine in the samples ranged from 19.66~54.97 mg/g. The method is easy, sensitive and accurate, and is suitable for the determination of nicotine in the tobacco concrete. |
| |
Keywords: | |
本文献已被 维普 等数据库收录! |
| 点击此处可从《分析测试技术与仪器》浏览原始摘要信息 |
| 点击此处可从《分析测试技术与仪器》下载免费的PDF全文 |
|