| 毛细管气相色谱法测定三聚氰酸三烯丙酯中丙烯醇的含量 |
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| 引用本文： | 蒋琴.毛细管气相色谱法测定三聚氰酸三烯丙酯中丙烯醇的含量[J].分析测试技术与仪器,2009,15(1):51-54. |
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| 作者姓名： | 蒋琴 |
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| 作者单位： | 南京大学,现代分析中心,江苏,南京,210093 |
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| 摘 要： | 建立了毛细管气相色谱测定三聚氰酸三烯丙酯中丙烯醇含量的方法．采用25m×0．32mm×0．25μm FFAP毛细管柱分离，氢火焰离子化检测器，内标标准曲线法（正丁醇作内标物）定量．方法简便、快速、准确，测定的相对标准偏差为0．61％～1．97％，平均回收率为97．1％～100．7％．
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| 关 键 词： | 毛细管气相色谱 三聚氰酸三烯丙酯 丙烯醇 |
Analysis of Allyl Alcohol in Triallyl Cyanurate by Capillary Column Gas Chromatography |
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| JIANG Qin.Analysis of Allyl Alcohol in Triallyl Cyanurate by Capillary Column Gas Chromatography[J].Analysis and Testing Technology and Instruments,2009,15(1):51-54. |
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| Authors: | JIANG Qin |
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| Institution: | Center of Materials Analysis;Nanjing University;Nanjing 210093;China |
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| Abstract: | A capillary column gas chromatographic method for the determination of allyl alcohol in triallyl eyanurate is described. The analysis was performed on an FFAP capillary column with GC- FID, using an internal standard method with n-C4H9OH as the internal standard, the average recoveries ranged from 97.1% - 100.7% with a relative standard deviations between 0. 61% - 1.97%. The method is simple, rapid and accurate with high reproducibility. |
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| Keywords: | capillary gas chromatography triallyl cyanurate allyl alcohol |
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