| 竹炭为高效吸附剂的固相萃取分析环境水样中的痕量三氯生 |
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| 引用本文： | 王霞,张莉莉,刁春鹏,赵汝松.竹炭为高效吸附剂的固相萃取分析环境水样中的痕量三氯生[J].分析试验室,2009,28(8). |
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| 作者姓名： | 王霞 张莉莉 刁春鹏 赵汝松 |
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| 作者单位： | 山东省分析测试中心,山东省大型精密分析仪器应用技术重点实验室,济南,250014 |
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| 基金项目： | 山东省重大科技专项基金，山东省优秀中青年科学家科研奖励基金 |
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| 摘 要： | 建立了一种由竹炭作为固相萃取高效吸附剂富集环境水样中痕量三氯生的新方法. 研究并优化了几个影响富集效率的参数. 在优化条件下, 三氯生的检测限为0.08 μg/L, 在1～100 μg/L 范围内有良好的线性关系, 相对标准偏差为2.9% (n=7). 方法可应用于实际废水样品的分析.
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| 关 键 词： | 竹炭 固相萃取 三氯生 环境水样 |
Bamboo charcoal as a solid-phase extraction adsorbent for enrichment and determination of triclosan in environmental water samples |
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| WANG Xia,ZHANG Li-li,DIAO Chun-peng,ZHAO Ru-song.Bamboo charcoal as a solid-phase extraction adsorbent for enrichment and determination of triclosan in environmental water samples[J].Chinese Journal of Analysis Laboratory,2009,28(8). |
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| Authors: | WANG Xia ZHANG Li-li DIAO Chun-peng ZHAO Ru-song |
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| Institution: | Key Laboratory for Applied Technology of Sophisticated Analytical Instruments of Shandong Province;Analysis and Test Center;Shandong Academy of Sciences;Jinan 250014 |
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| Abstract: | In this article, a new method based on using bamboo charcoal as a solid-phase extraction adsorbent for the enrichment and determination of triclosan has been developed. Several related factors that may influence the enrichment efficiency were investigated and optimized in detail. Under the optimum conditions, the limit of detection was 0.08 μg/L. There was good linearity (R2=0.9969) over the range 1～100 μg/L and good reproducibility with relative standard deviation of 2.9% (n=7). The proposed method has been applied to the analysis of real wastewater samples and satisfactory results were obtained. |
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| Keywords: | Bamboo charcoal Solid-phase extraction Triclosan Environmental water samples |
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