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佩兰挥发性化学成分的固相微萃取研究
引用本文:杨再波,钟才宁,孙成斌,毛海立.佩兰挥发性化学成分的固相微萃取研究[J].分析试验室,2008,27(1):84-87.
作者姓名:杨再波  钟才宁  孙成斌  毛海立
作者单位:黔南民族师范学院化学系,都匀,558000
摘    要:采用固相微萃取-气相色谱-质谱法分析佩兰中挥发性化学成分,共分离出84个组分,并鉴定了67个组分,用归一化法测定其质量分数,占总挥发性组分峰面积的98.05%。主要成分是对-伞花烃(5.19%)、芳樟醇(3.72%)、β-石竹烯(12.35%)、α-律草烯(13.39%)、α-姜黄烯(2.11%)、(-)-石竹烯氧化物(8.25%)、. /-.-4-乙酰基-1-甲基环己烯(8.91%)。

关 键 词:佩兰  挥发油  化学成分  固相微萃取  气相色谱-质谱
文章编号:1000-0720(2008)01-084-04
收稿时间:2006-09-28
修稿时间:2006-12-08

Study on chemical constituents of the volatile oils from eupatorium fortunei turcz by SPME
YANG Zai-bo,ZHONG Cai-ning,SUN Cheng-bin,MAO Hai-li.Study on chemical constituents of the volatile oils from eupatorium fortunei turcz by SPME[J].Chinese Journal of Analysis Laboratory,2008,27(1):84-87.
Authors:YANG Zai-bo  ZHONG Cai-ning  SUN Cheng-bin  MAO Hai-li
Institution:Department of Chemistry;Qiannan Normal University for Nationalities;Duyun 558000
Abstract:The chemical components of volatile oils from eupatorium fortunei turcz were analyzed by SPME-GC-MS.84 components were separated in the total volatile oil and 67 components were identified by GC-MS.Their contents were determined by normalization method.The contents of the identified compounds add up to about 98.05% of the total volatile oils.Among them,the main chemical components are p-cymene(5.19%),linalool(3.72%),beta-Caryophyllene(12.35%),alpha-humulene(13.39%),alpha-curcumene(2.11%),(-)-Caryophyllene oxide(8.25%), /-.-4-Acetyl-1-methylcyclohexene(8.91%).
Keywords:Eupatorium fortunei  Volatile oil  Chemical components  SPME  GC-MS
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