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酸枣仁中挥发性化学成分分析
引用本文:侯冬岩,回瑞华,杨梅,李铁纯,郭华.酸枣仁中挥发性化学成分分析[J].分析试验室,2003,22(3):84-86.
作者姓名:侯冬岩  回瑞华  杨梅  李铁纯  郭华
作者单位:1. 鞍山师范学院化学系,鞍山,114005;辽宁师范大学化学系,大连,116029
2. 辽宁师范大学化学系,大连,116029
3. 鞍山师范学院化学系,鞍山,114005
基金项目:辽宁省教育厅科学技术基金资助课题 (No .2 0 3310 79)
摘    要:报道了用蒸馏-萃取法提取酸枣仁中挥发性物质,测得酸枣仁挥发油的含量为10.40%,用GC/MS法从酸枣果肉挥发油中分离并确定出38种化学成分。用峰面积归一化法通过化学工作站数据处理系统,得出各化学成分在挥发油中的含量。其中主要成分为酯类化合物占挥发油总量的76.12%,其次为酸类化合物为7.65%,醇类化合物为3.43%,醚类化合物为2.16%,烷烃化合物为4.61%,其它类化合物仅占4.85%。共占酸枣仁中挥发油总量的98.82%。

关 键 词:酸枣仁  挥发性化学成分  分析  蒸馏-萃取法  提取  挥发油  气相色谱-质谱
文章编号:1000-0720(2003)03-0084-03

Studies on volatile constituents of seed in zizyphusjujuba mill
HOU Dong-yan ,HUI Rui-hua ,YANG Mei,LI Tei-chun and GUO Hua.Studies on volatile constituents of seed in zizyphusjujuba mill[J].Chinese Journal of Analysis Laboratory,2003,22(3):84-86.
Authors:HOU Dong-yan    HUI Rui-hua    YANG Mei  LI Tei-chun and GUO Hua
Institution:HOU Dong-yan *1,2,HUI Rui-hua 1,2,YANG Mei2,LI Tei-chun1 and GUO Hua1
Abstract:The water distillation-extractor was used for extracting the volatile substances of the seed in Zizyphusjujuba Mill. The average oil yield obtained was 10.40%. 38 chemical components were identified by gas chromatography/massspectrometry (GC/MS) method. Of them the main components are: esters(76.12%), acids (7.65% ), alcohols (3.43%), ethers (2.16%), aliphatic compounds (4.61%) and others (4.85%). The contents of the identified compounds make up 98.82% of the total volatile substances detected.
Keywords:Seed of zizyphusjujuba mill  Volatile substances  Water distillation-extractor  Gas chromatography/Mass spectrometry
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