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顶空毛细管柱气相色谱法测定水中的二氯甲烷
引用本文:陈妍妍,杨丽莉.顶空毛细管柱气相色谱法测定水中的二氯甲烷[J].化学分析计量,2005,14(6):47-48.
作者姓名:陈妍妍  杨丽莉
作者单位:南京市环境监测中心站,南京,210013;南京市环境监测中心站,南京,210013
摘    要:采用毛细管柱分离、顶空气相色谱法测定水中的二氯甲烷,讨论了恒温平衡时间和盐效应对气液平衡的影响。该方法检出限为0.001 mg/L,二氯甲烷的加标回收率为87.7%~110%,测定结果的相对标准偏差为6.2%~8.7%(n=6)。

关 键 词:顶空气相色谱法  毛细管柱  二氯甲烷  
修稿时间:2005年9月12日

DETERMINATION OF DICHLOROMETHANE IN WATER BY HEADSPACE GAS CHROMATOGRAPHY
Chen Yanyan,Yang Lili.DETERMINATION OF DICHLOROMETHANE IN WATER BY HEADSPACE GAS CHROMATOGRAPHY[J].Chemical Analysis And Meterage,2005,14(6):47-48.
Authors:Chen Yanyan  Yang Lili
Abstract:The headspace gas chromatographic method was used to determine dichloromethane in water.The influence of the time and salt effect to the gas-liquid balance were discussed.The detection limit of dichloromethane was 0.001 mg/L,the relative standard deviation were 6.2%-8.7% and the recoveries were 87.7%-110%.
Keywords:headspace gas chromatography  capillary column  dichloromethane  water
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