| HPLC-DAD法测定猪肝中的盐酸克伦特罗 |
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| 引用本文： | 刘平年.HPLC-DAD法测定猪肝中的盐酸克伦特罗[J].化学分析计量,2005,14(5):33-35. |
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| 作者姓名： | 刘平年 |
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| 作者单位： | 上海市食品研究所检测中心,上海,200235 |
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| 摘 要： | 建立了用5％高氯酸溶液酸化提取，SCX固相小柱净化，高效液相色谱（HPLC）法测定猪肝中的盐酸克伦特罗的方法，利用二极管阵列检测器（DAD）定量并辅助定性。该方法的平均加标回收率为79％，检出限为0．01mg／kg。
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| 关 键 词： | 盐酸克伦特罗 高效液相色谱法 二极管阵列检测器 固相萃取 |
| 修稿时间： | 2005年6月30日 |
ANALYSIS OF CLENBUTEROL IN PORK LIVER BY HPLC-DAD |
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| Liu Pingnian.ANALYSIS OF CLENBUTEROL IN PORK LIVER BY HPLC-DAD[J].Chemical Analysis And Meterage,2005,14(5):33-35. |
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| Authors: | Liu Pingnian |
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| Abstract: | A high performance liquid chromatography method for the determination of Clenbuterol in pork liver was established.The sample was treated with 5% HClO_(4) solution,extracted and purified by SCX column,and analyzed by HPLC-DAD.Diode array detector was used for qualitification and quantification.The average recovery was 79%,the detection limit of this method was(0.01) mg/kg. |
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| Keywords: | clenbuterol HPLC DAD SPE |
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