| 超临界CO_2萃取-分子蒸馏对大蒜化学成分的提取与分离 |
| |
| 引用本文： | 张忠义, 雷正杰, 王鹏, 吴惠勤.超临界CO_2萃取-分子蒸馏对大蒜化学成分的提取与分离[J].分析测试学报,2002,21(1):65-67. |
| |
| 作者姓名： | 张忠义 雷正杰 王鹏 吴惠勤 |
| |
| 作者单位： | 第一军医大学珠江医院,广东,广州,510282 |
| |
| 基金项目： | 广东省2000年科技攻关项目 (2KBO1202S) |
| |
| 摘 要： | 采用超临界CO2流体萃取技术和分子蒸馏对大蒜化学成分进行萃取与分离，用气相色谱－质谱联用技术测定其化学成分；从超临界CO2萃取物中鉴定出16种成分，经分子蒸馏后，得到4种主要成分：二烯丙基二硫、3－乙烯基－1，2－二硫代环己－5－烯、2－乙烯基－1，3－二硫代环己－5－烯及二烯丙基三硫。
|
| 关 键 词： | 大蒜 超临界流体萃取 分子蒸馏 超临界二氧化碳 化学成分 提取 气相色谱 质谱 分离 分析 |
| 文章编号： | 1004-4957(2002)01-0065-03 |
| 修稿时间： | 2001年3月15日 |
Studies on Chemical Composition of Garlic by Supercritical CO2 Fluid Extraction and Molecular Distillation |
| |
| ZHANG Zhong _ yi,LEI Zheng _ jie,WANG Peng,WU Hui _ qin.Studies on Chemical Composition of Garlic by Supercritical CO2 Fluid Extraction and Molecular Distillation[J].Journal of Instrumental Analysis,2002,21(1):65-67. |
| |
| Authors: | ZHANG Zhong _ yi LEI Zheng _ jie WANG Peng WU Hui _ qin |
| |
| Institution: | ZHANG Zhong _ yi1,LEI Zheng _ jie1,WANG Peng1,WU Hui _ qin2 |
| |
| Abstract: | Chemical components of garlic were extracted by supercritical CO2 fluid and separated by molecular distillation(MD). The extractive and distillate were analyzed by gas chromatography-mass spectrometry. 16 compounds in the extractive were identified, whereas 4 compounds are obtained by molecular distillation of the extractive. They are diallyl disulfide, 3 _ ethenyl _ 1,2 _ dithia _ cyclohex _ 5 _ ene, 2 _ ethenyl _ 1,3 _ dithia _ cyclohex _ 5_ ene and diallyl trisulfide. |
| |
| Keywords: | Garlic Supercritical fluid extraction Molecular distillation |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《分析测试学报》浏览原始摘要信息 |
| 点击此处可从《分析测试学报》下载免费的PDF全文 |
