| 金汞齐富集冷原子荧光测汞法的研究 |
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| 引用本文： | 刘买利,李晓玲,牛深克,杜文虎.金汞齐富集冷原子荧光测汞法的研究[J].分析测试学报,1989(2). |
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| 作者姓名： | 刘买利 李晓玲 牛深克 杜文虎 |
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| 作者单位： | 西北大学分析测试研究中心
(刘买利，李晓玲)，西安交通大学
(牛深克)，西北大学分析测试研究中心(杜文虎) |
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| 摘 要： | 本文介绍了一种用于测定汞的金汞齐富集热解系统。研究了该系统与冷原子荧光测汞仪联用的工作条件和干扰,在最佳条件下的检出下限为4×10~(-13)克汞,分析周期3分钟,相对标准偏差2.5%(1.5×10~(-9)克汞)。
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| 关 键 词： | 汞 金汞齐富集 冷原子荧光测汞法 |
Datermination of Meacury by Non-Dispersive Atomic Fluorescence Spectrometer With Gold Amalgamation Concentration |
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| Liu Maili,Li Xiaolihg,NiuShenke,Du Wenhu Instrumental Analysis and Resgarch Center Northwestern University.Datermination of Meacury by Non-Dispersive Atomic Fluorescence Spectrometer With Gold Amalgamation Concentration[J].Journal of Instrumental Analysis,1989(2). |
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| Authors: | Liu Maili Li Xiaolihg NiuShenke Du Wenhu Instrumental Analysis and Resgarch Center Northwestern University |
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| Institution: | Liu Maili;Li Xiaolihg;NiuShenke;Du Wenhu Instrumental Analysis and Resgarch Center Northwestern University |
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| Abstract: | A non-dispersive atomic fluorescence system determining mercury which makesuse of Au-coated chromatographic supports for collection of Hg and a water-coolingelectric furnace for desorption of Hg are described. The experimental conditions andthe effects of some organic solvents vapour on determination of Hg have been investi-gated. After optimization the detection limit of 0.0004 ng of Hg, the relative standarddeviation of 2.5%(1.5 ng of Hg, n=10) and the cycle time of 3 min. for entireprocese are obtained. Results are reported for application of the system to a varietyof samples, including gases, liquids and solids. |
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| Keywords: | Mercury gold amalglamation non-dispersive atomic fluoresence spectrometry |
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