| 气相色谱法测定生物柴油样品中脂肪酸甲酯和脂肪酸甘油酯的含量 |
| |
| 引用本文： | 李长秀, 唐忠, 杨海鹰.气相色谱法测定生物柴油样品中脂肪酸甲酯和脂肪酸甘油酯的含量[J].分析测试学报,2005,24(5):66-68. |
| |
| 作者姓名： | 李长秀 唐忠 杨海鹰 |
| |
| 作者单位： | 1. 中国石化股份公司,石油化工科学研究院,北京,100083
2. 中国石化股份公司,金陵分公司,江苏,南京,210033 |
| |
| 摘 要： | 建立了气相色潜测定生物柴油样品中脂肪酸甘油酯的方法、该方法不需对样品进行衍生化处理，以耐高温的毛细管柱作分析柱，采用冷柱头柱上进样，氢火焰离予化检测器检测，内标法定量，直接得到生物柴油制备工艺所得产物中脂肪酸甲酯、脂肪酸甘油单酯、甘油二酯和甘油三酯的含量。
|
| 关 键 词： | 生物柴油 脂肪酸甘油酯 气相色谱 |
| 文章编号： | 1004-4957（2005）05-0066-03 |
| 收稿时间： | 2004-08-08 |
| 修稿时间： | 2004-12-08 |
Determination of Fatty Acid Methyl Esters and Glycerides in Bio- diesel Samples by GC |
| |
| LI Chang-xiu,TANG Zhong,YANG Hai-ying.Determination of Fatty Acid Methyl Esters and Glycerides in Bio- diesel Samples by GC[J].Journal of Instrumental Analysis,2005,24(5):66-68. |
| |
| Authors: | LI Chang-xiu TANG Zhong YANG Hai-ying |
| |
| Abstract: | A gas chromatographic method is developed for the detemlination of fatty acid methyl esters and glycerides in bio-diesel samples. A non-polar capillary column of high temperature tolerance was used for separation. The sample was introduced via the cool on-column injector and detected by the flame ionization detector without pre-derivation. The intenal standard method was used for quantificatioll. The method is simple and rapid and can be used for the determination of the conversion rate of fatty acid glycerides in the preparation process of bio-dxiesel. |
| |
| Keywords: | Bio-diesels Fatty acid glycerides Gas chromatography |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《分析测试学报》浏览原始摘要信息 |
| 点击此处可从《分析测试学报》下载免费的PDF全文 |
