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色谱法分离富勒烯的研究
引用本文:张宝,李新海.色谱法分离富勒烯的研究[J].分析测试学报,1998,17(1):70-72.
作者姓名:张宝  李新海
作者单位:中南工业大学冶金物理化学与化学新材料研究所
摘    要:研究了用活性炭作固定相,CS2作流动相柱色谱法分离富勒烯混合物的方法,考察了用溶剂浸泡活性炭减活的时间、活性炭与富勒烯混合物配比、活性炭的粒度等因素对分离结果的影响,采用了索氏抽提器,可以很快地将固定相中的C70等高级富勒烯提取出来,提高了回收率。

关 键 词:富勒烯,液相色谱,分离,索氏抽提

Study on Liquid Chromatographic Separation of Fullerenes
Zhang Bao,Li Xinhai,Wang Zhixing,Li Jing.Study on Liquid Chromatographic Separation of Fullerenes[J].Journal of Instrumental Analysis,1998,17(1):70-72.
Authors:Zhang Bao  Li Xinhai  Wang Zhixing  Li Jing
Abstract:For chromatographic separation of fullerenes, a method in which active cabon was used as stantionary phase and CS 2 as mobile phase was studied by the authors and the influence on separation of solvent leaching time for deactivating active carbon, ratio of active carbon to fullerenes and particle size of active carbon were investigated. By using Soxhlet extractor, the C 70 and other higher fullerenes can be quickly extracted from the stationary phase with a higher yield.
Keywords:Fullerene  Liquid chromatographic Separation  Soxhlet extractor
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