| 水果、蔬菜中16种有机氯残留农药的毛细管气相色谱测定法 |
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| 引用本文： | 余建新, 邵俊杰, 胡小钟, 孙保国, 吴采樱.水果、蔬菜中16种有机氯残留农药的毛细管气相色谱测定法[J].分析测试学报,1999,18(3):29-32. |
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| 作者姓名： | 余建新 邵俊杰 胡小钟 孙保国 吴采樱 |
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| 作者单位： | 1. 湖北进出口商品检验局,武汉,430022
2. 武汉大学化学学院,武汉,430072 |
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| 摘 要： | 采用柱层析净化方式，以ＨＰ－１０１弹性石英毛细管柱为分离柱，电子捕获检测的气相色谱法测定水果、蔬菜中１６种有机氯农药残留量。方法的检出限为０．１×１０－９～２．０×１０－９，回收率范围在８７．５％～１０６．３％之间，相对标准偏差为３．０％～９．５％。
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| 关 键 词： | 有机氯农药 残留 电子捕获检测器 气相色谱法 |
Determination of Residues of 16 Organochloride_containing Pesticides in Fruits,Vegetable by GC Method |
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| Yu Jianxin,Shao Junjie,Hu Xiaozhong,Sun Baoguo,Wu Caiying.Determination of Residues of 16 Organochloride_containing Pesticides in Fruits,Vegetable by GC Method[J].Journal of Instrumental Analysis,1999,18(3):29-32. |
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| Authors: | Yu Jianxin Shao Junjie Hu Xiaozhong Sun Baoguo Wu Caiying |
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| Abstract: | Residues of 16 organochloride pesticides in fruits and vegetables have been determined by GC-ECD with HP-101 crosslinked capillary column. The detection limits of the method are in 0.110-92.010-9, recoveries in 87.56.3% and relative standard deviation in 3.0%9.5%. |
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| Keywords: | Organochloride pesticide Residue GC-ECD |
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