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GC/MS SIM法快速测定酒中的游离脂肪酸
引用本文:程誌青,吴惠勤.GC/MS SIM法快速测定酒中的游离脂肪酸[J].分析测试学报,1992(6).
作者姓名:程誌青  吴惠勤
作者单位:中国广州分析测试中心 广州 (程誌青),中国广州分析测试中心 广州(吴惠勤)
摘    要:本文介绍一种简单、快速、灵敏、直接分析酒中游离脂肪酸的测定方法。用涂有OV-17熔融石英毛细管柱。选择游离脂肪酸质谱图中的基峰离子m/z 60进行SIM检测。定量测定了茅台酒、珍酒及鸭溪窖酒中十二种游离脂肪酸。

关 键 词:GC/MS  SIM法  游离脂肪酸

Rapid Determination of Free Fatty Acids in Wine by GC/MS SIM
Cheng Zhiqing,Wu Huiqin Guangdong Institute of Analysis.Rapid Determination of Free Fatty Acids in Wine by GC/MS SIM[J].Journal of Instrumental Analysis,1992(6).
Authors:Cheng Zhiqing  Wu Huiqin Guangdong Institute of Analysis
Institution:Cheng Zhiqing;Wu Huiqin Guangdong Institute of Analysis
Abstract:A simple, rapid and sensitive method for direct determination of free fatty acids in wineswas described by the authors. It is accomplished on a fused quartz capillary column coated withOV-17. The ion m/z 60 of the base peak in the mass of spectrum of C_4-C_(18) normal fatty acidswas used in GC/MS SIM. The contents of 12 free fatty acids in Maotai, Rare Distillate andYaxijiaojiu have been determined by this method.
Keywords:Free fatty acid  Wine  GC/MS  SIM  
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