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微波加热快速测定腐植酸总量
引用本文:高岐,王翠.微波加热快速测定腐植酸总量[J].分析测试学报,1994,13(2):74-78.
作者姓名:高岐  王翠
作者单位:河南农业大学基础部,河南省职业病防治所
摘    要:利用微波加热技术,在密闭容器内通过压力浸提、消解试样、能大大加快分析速度,本实验测定了不同煤样中的腐植酸总量,讨论了功率、时间、酸度等因素对分析结果的影响,并与标准方法相对照,用t-检验法及F-检验法检验,没有明显差异,结果令人满意,该法具有省时、省力、经济、不污染环境,宜于批量分析,便于普及推广等优点。

关 键 词:微波加热  腐植酸  浸提  测定

Rapid Determination of the Total Content of the Humic Acid in Coal Samples by Using
Microwave-Heating Method Gao Qi, Gao Xiangyang, Huang Xiaoshu.Rapid Determination of the Total Content of the Humic Acid in Coal Samples by Using[J].Journal of Instrumental Analysis,1994,13(2):74-78.
Authors:Microwave-Heating Method Gao Qi  Gao Xiangyang  Huang Xiaoshu
Abstract:Using microwave-heating method, coal samples were digested with sodium pyrophoshatesodium hydroxide and were dispelled with potassium bichromate-sulfuric acid in the closed vessel.This paper has discussed the effect of analysis result by power, time and acidity etc.In different coal sample, humic acid amount was measured. Compared with classical method, Using t-test and F-test the result is satisfactory. This method has many advantages such as saving time, saving labour, saving money and not polluting environment.This method is appropriate for batch analysis and easy to spread.
Keywords:Microwave-heating  Humic acid  Digestion  
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