| (5-甲基-2-烷氧基苯基)-1-烃基胺的合成 |
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| 引用本文： | 刘改玲,姜岚,李争宁.(5-甲基-2-烷氧基苯基)-1-烃基胺的合成[J].合成化学,2012,20(2):186-192. |
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| 作者姓名： | 刘改玲 姜岚 李争宁 |
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| 作者单位： | 1. 大连大学环境与化工学院,辽宁大连,116622
2. 大连大学环境与化工学院,辽宁大连116622;大连大学辽宁省生物有机化学重点实验室,辽宁大连116622 |
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| 基金项目： | 国家自然科学基金资助项目 |
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| 摘 要： | 以对甲酚(1)为起始原料,经醚化、酰化和还原氨化反应合成了5个(5-甲基-2-乙氧基苯基)-1-烃基胺；1经酯化、Fries重排、醚化和还原氨化反应合成了5个(5-甲基-2-甲氧基苯基)-1-烃基胺.其结构经1H NMR,13C NMR,IR和GC-MS表征.
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| 关 键 词： | 胺 (5-甲基-2-烷氧基苯基)-1-烃基胺 还原氨化 合成 |
Synthesis of 1-(2-Alkoxyl-5-methylphenyl)alkylamine |
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| LIU Gai-ling
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JIANG Lan
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LI Zheng-ning.Synthesis of 1-(2-Alkoxyl-5-methylphenyl)alkylamine[J].Chinese Journal of Synthetic Chemistry,2012,20(2):186-192. |
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| Authors: | LIU Gai-ling JIANG Lan LI Zheng-ning |
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| Institution: | 1a,1b(a.College of Environmental and Chemical Engineering; b.Liaoning Key Laboratory of Bioorganic Chemistry,1.Dalian University,Dalian 116622,China) |
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| Abstract: | Five 1-(2-ethoxy-5-methylphenyl)-alkylamines were synthesized from 4-cresol(1) by etherification,acylation and reductive amination.Five 1-(2-methoxyl-5-methylphenyl)-alkylamines were synthesized from 1 by esterification,Fries rearrangement,esterification and reductive amination.The structures were characterized by 1H NMR,13C NMR,IR and GC-MS. |
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| Keywords: | amine 1-(2-alkoxyl-5-methylphenyl)-alkylamine reductive amination synthesis |
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