日香桂根的化学成分研究(III) |
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引用本文: | 张旭,秦玉琴,张春艳,李羽晗,石继祥,王欣,陆世惠,黄静.日香桂根的化学成分研究(III)[J].合成化学,2016(8):728-731. |
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作者姓名: | 张旭 秦玉琴 张春艳 李羽晗 石继祥 王欣 陆世惠 黄静 |
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作者单位: | 四川大学华西药学院,四川成都,610041 |
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摘 要: | 利用柱层析法(硅胶,C18)从日香桂根的乙酸乙酯提取物中分离出8个单体化合物女贞苷(1),连翘苷(2),(+)-羟基松脂醇-1-O-β-D-葡萄糖(3),(+)-环橄榄树脂素(4),2α,3β-二羟基乌苏-12-烯-28酸(5),对羟基苯乙醇(6),(-)-橄榄脂素(7)和橄榄树脂素-4-O-β-D-葡萄糖苷(8)],其结构经1 H NMR和13 C NMR确证。5为首次在木犀科植物中发现,4为首次在木犀属植物中发现,2,3,7和8为首次在日香桂植物中发现。
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关 键 词: | 木犀科 木犀属 日香桂 柱层析法 化学成分 |
Studies on the Chemical Components of the Roots of Osmanthus fragrans ‘Rixianggui’ (III) |
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Abstract: | The chemical components of the roots of Osmanthus fragrans‘Rixianggui’ were investigated by the chromatography methods(silica gel, C18).Eight compoundsligustroside (1), phillyrin(2), (+)-hydroxyinoresinol-1-O-β-D-glucoside ( 3 ) , ( +)-cyclo-olivil ( 4 ) , 2 , 3-dihydroxyurs-12-en-28-oic acid(5), p-hydroxyphenylethanol(6), ( -)-olivil(7) and ( -)-olivil-4-O-β-D-glucopyranoside (8)] were isolated from the EA extract of the roots of the title plant.The structures were confirmed by 1 H NMR and 13 C NMR.5 was isolated from the family Oleaceae, 4 from genus Osmanthus and 2, 3, 7, 8 from this plant for the first time. |
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Keywords: | Oleaceae Osmanthus fragrans Rixianggui chromatography method chemical constituent |
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