| N,N-二甲基乙醇胺三个季铵盐衍生物的合成与表征 |
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| 引用本文： | 张学同,周贵忠,廖双泉,罗运军,谭惠民.N,N-二甲基乙醇胺三个季铵盐衍生物的合成与表征[J].合成化学,2002,10(5):451-453. |
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| 作者姓名： | 张学同 周贵忠 廖双泉 罗运军 谭惠民 |
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| 作者单位： | 北京理工大学化工与材料学院,北京,100081 |
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| 摘 要： | 以N，N－二甲基甲酰胺为溶剂，乙酸乙酯为催化剂，N，N－二甲基乙醇胺分别与苄基氯、十二烷基溴和十八烷基溴作用，得到了3个N，N－二甲基乙醇胺的季铵盐衍生物。标题化合物结构经IR，^1H NMR,^13C NMRt FAB-MS表征。
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| 关 键 词： | 衍生物 合成 表征 N，N－二甲基乙醇胺 季铵盐 苄基氯 十二烷基溴 十八烷基溴 |
Synthesis and Characterization of Three Derivatives of Quaternary Ammonium Salts of N,N-dimethyl Ethanolamine |
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| ZHANG Xue-tong,ZHOU Gui-zhong,LIAO Shuang-quan,LUO Yun-jun,TAN Hui-min.Synthesis and Characterization of Three Derivatives of Quaternary Ammonium Salts of N,N-dimethyl Ethanolamine[J].Chinese Journal of Synthetic Chemistry,2002,10(5):451-453. |
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| Authors: | ZHANG Xue-tong ZHOU Gui-zhong LIAO Shuang-quan LUO Yun-jun TAN Hui-min |
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| Abstract: | Three derivatives of quaternary ammonium salts of ethanolamine were synthesized by the reaction of N,N-dimethyl ethanolamine with benzyl chloride, lauryl bromide and octadecyl bromide, respectively. The synthesis was conducted in the presence of DMF with ethyl acetate as a catalyst. Molecular structures of the derivatives were determined by IR, 13C NMR, 1H NMR and MS. |
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| Keywords: | N N-dimethyl ethanolamine quaternary ammonium salt benzyl chloride lauryl bromide octadecyl bromide |
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