| 2-烷硫基-5-苯基亚甲基-4H-咪唑啉-4-酮的合成与表征 |
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| 引用本文： | 孙勇,丁明武.2-烷硫基-5-苯基亚甲基-4H-咪唑啉-4-酮的合成与表征[J].合成化学,2003,11(6):469-471,498. |
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| 作者姓名： | 孙勇 丁明武 |
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| 作者单位： | 1. 郧阳师范高等专科学校化学系,湖北,丹江口,442700
2. 华中师范大学化学学院有机合成研究所,湖北,武汉,430079 |
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| 基金项目： | 国家自然科学基金资助项目(20102001);湖北省教育厅自然科学基金(2003A002)资助项目 |
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| 摘 要： | 用2-硫代-3-正丁基-5-苯基亚甲基4-咪唑啉二酮的-S-烷基化反应合成了2-烷硫基-3-正丁基-5-苯基亚甲基-4H-咪唑啉-4-酮衍生物。探讨了S-烷基化反应的反应条件和所合成化合物的波谱性质。目标产物均为新的化合物，其结构经元素分析，IR，1H NMR和MS确正。
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| 关 键 词： | 2-硫代-4-咪唑啉二酮 4H-咪唑啉-4-酮 S-烷基化 合成 |
| 文章编号： | 1005-1511(2003)06-0469-03 |
Synthesis and Characterization of 2-Alkylthio-5-phenylmethylidene-4H-imidazolin-4-ones |
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| SUN Yong ,DING Ming-wu.Synthesis and Characterization of 2-Alkylthio-5-phenylmethylidene-4H-imidazolin-4-ones[J].Chinese Journal of Synthetic Chemistry,2003,11(6):469-471,498. |
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| Authors: | SUN Yong DING Ming-wu |
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| Institution: | SUN Yong 1,DING Ming-wu 2 |
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| Abstract: | 2-Alkylthio-3-(n-butyl)-5-phenylmethylidene-4H-imidazolin-4-ones were synthesized by S-alkylation of 2-thio-3-(n-butyl)-5-phenylmethylidene-4-imidazolidinone. The conditions of S-alkylation reaction and the spectral properties of the synthesized compounds were researched. All the synthesized products are new, and their structures were confirmed by elemental analysis, IR, 1H NMR and MS. |
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| Keywords: | 2-thio-4-imidazolidinone 4H-imidazolin-4-ones S-alkylation synthesis |
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