| 二烃基锡双（O，O－二硫代磷酸酯）的合成和波谱研究 |
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| 引用本文： | 谢庆兰,朱应怀,杨志强. 二烃基锡双（O，O－二硫代磷酸酯）的合成和波谱研究[J]. 合成化学, 1996, 0(3) |
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| 作者姓名： | 谢庆兰 朱应怀 杨志强 |
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| 作者单位： | 南开大学元素有机化学实验室，元素有机化学研究所 |
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| 摘 要： | 合成了１５个二烃基双（Ｏ，Ｏ－二硫代磷酸酯）化合物。利用ＩＲ、（１Ｈ、１３Ｃ、１１９Ｓｎ）ＮＭＲ表征了化合物的结构。这是一类六配位变形八面体结构的二烃基锡化合物。对化合物的质谱裂解机制进行了讨论。
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| 关 键 词： | 二烃基锡 二硫代磷酸酯 结构表征 |
Preparation and Characterization of (O,O dialkyl dithiophosphato)dialkyltin Compounds |
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| Xie,Qing Lan Zhu,Ying Huai Yang,Zhi Qiang. Preparation and Characterization of (O,O dialkyl dithiophosphato)dialkyltin Compounds[J]. Chinese Journal of Synthetic Chemistry, 1996, 0(3) |
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| Authors: | Xie Qing Lan Zhu Ying Huai Yang Zhi Qiang |
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| Abstract: | Fifteen bis(O,O dialkyl dithiophosphato)dialkyltin were prepared and their structures were characterized through IR, ( 1H, 13 C, 119 Sn) NMR. The compound has a tin atom in a distorted six coordination octahedron and two anisobidentated dithiophosphate ligands. The breakdown pattern of MS were also discussed. |
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| Keywords: | Dialkyltin Dithiophosphate Structural characterization. |
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