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2,4,6-三硝基苯腙的合成及其抑菌活性
引用本文:范铮,单尚.2,4,6-三硝基苯腙的合成及其抑菌活性[J].合成化学,2006,14(3):275-277.
作者姓名:范铮  单尚
作者单位:1. 浙江工业大学生物与环境学院,浙江,杭州310014;浙江工业大学,化工与材料学院,浙江,杭州310014
2. 浙江工业大学化工与材料学院,浙江,杭州310014
摘    要:三硝基氯苯与水合肼反应,直接合成了2,4,6-三硝基苯肼(2),2与醛、酮试剂反应合成了6个新的苯腙化合物,其结构经1H NMR,IR和元素分析表征。抑菌试验表明,部分目标产物具有良好的抑菌活性。

关 键 词:间三硝基苯腙  合成  抑菌活性
文章编号:1005-1511(2006)03-0275-03
收稿时间:2005-12-26
修稿时间:2005年12月26

Synthesis of 2,4,6-Trinitrophenylhydrazones and Their Antibacterial Activity
FAN Zheng,SHAN Shang.Synthesis of 2,4,6-Trinitrophenylhydrazones and Their Antibacterial Activity[J].Chinese Journal of Synthetic Chemistry,2006,14(3):275-277.
Authors:FAN Zheng  SHAN Shang
Institution:1,College of Biology and Environment, b. College of Chemical Engineering and Materials, 2, Zhejiang University of Technology, Hangzhou 310014, China
Abstract:Six novel 2,4,6-trinitrophenylhydrazones in the yields of 63%~83% were synthesized by reaction of aldehyde(or ketone) with trinitrophenylhydrazine which was prepared from trinitro-chlorobenzene and hydrazine hydrate.The structures were confirmed by ~1H NMR,IR and elemental analysis.The antibacterial tests showed that some of 2,4,6-trinitrophenylhydrazones exhibited antibacterial activities.
Keywords:trinitrophenylhydrazone  synthesis  antibacterial activity
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