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Radicals in organic synthesis: part 2

Authors:	Gareth J Rowlands [Author Vitae]

Institution:	Institute of Fundamental Sciences—Chemistry, Massey University, Private Bag 11 222, Palmerston North, New Zealand

Abstract:

Keywords:	ABCVA 4 4&prime -azobis(4-cyanovaleric acid) (VA-501) Ac acetyl ACCN 1 1&prime -azobis(cyclohexanecarbonitrile) (V-40 or VAZO-88) AIBN azobisisobutyronitrile Ar aryl ATRA atom transfer radical addition ATRC atom transfer radical cyclisation ATRP atom transfer radical polymerisation bipy 2 2&prime -bipyridine Bn benzyl BTAC benzyltriethylammonium chloride Bu butyl Bz benzoyl CAN cerium(IV) ammonium nitrate or ceric ammonium nitrate or diammonium cerium(IV) nitrate Cp cyclopentadienyl CTAB cetyltrimethylammonium bromide DCP dicumyl peroxide DEPO diethylphosphine oxide dHbipy 4 4&prime -di-n-heptyl-2 2&prime -dipyridyl DLP dilauroyl peroxide or lauroyl peroxide or dodecanoyl peroxide DMA N N-dimethylacetamide DMF dimethylformamide DMP 1 4-dimethylpiperazine DMSO dimethylsulfoxide EDC 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride EH 2-ethylhexanoate EPHP 1-ethylpiperidinium hypophosphite Et ethyl Fmoc 9-fluorenylmethoxycarbonyl h hour HMPA hexamethylphosphoramide HOBt 1-hydroxybenzotriazole HWE Horner-Wadsworth-Emmons IBX 1-hydroxy-1 2-benziodoxol-3(1H)-one 1-oxide iPr isopropyl MAP 4-methoxyacetophenone Me methyl min minute(s) MOM methoxymethyl MS molecular sieves MW microwave Ph phenyl PMB para-methoxybenzyl PMDETA N N N&prime N&Prime N&Prime -pentamethyldiethylenetriamine PMP para-methoxyphenyl PRC polarity-reversal catalyst/catalysis PRE persistent-radical effect RCM ring-closing metathesis SET single electron transfer SEM 2-(trimethylsilyl)methoxymethyl TBDPS tert-butyldiphenylsilyl TBHN di-tert-butyl hyponitrite TBHP tert-butyl hydrogen peroxide TBPP tert-butyl peroxypivalate TBS tert-butyldimethylsilyl TBST tri-tert-butoxysilanethiol TBTH tributyltin hydride TEMPO 2 2 6 6-tetramethylpiperidine-1-oxyl radical Tf trifluoromethanesulfonyl or triflyl THP tetrahydropyran TMEDA N N N&prime N&prime -tetramethylethylenediamine TMS trimethylsilyl Tr trityl Ts toluenesulfonyl or tosyl TSE 2-tosylethyl TTMSS tris(trimethylsilyl)silane
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